User:Raquel Lara/Notebook/481-2018/2018/09/07

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Objective

  • Prepare standard samples from the standard solution of 100μg/mL and density 1.036 g/mL
  • Take ICP of prepared standards

Description

  1. Add experimental record here. Include what, how, and why...

Data

Concentration of standard

  • (100 μg/mL)(1 mL/1.036)= 96.5ppm
  • Stock solution of 1ppm made to be used for the ppb samples
    • (1ppm)(50g)=(96.5ppm)(X)
    • X= 0.51813g
  1. Actual Concentration of 1ppm Stock/Prepartation
    1. 0.514g of 96.5ppm standard
    2. water added to 50.3297g
    3. Actual Concentration: 985.5ppb

Standard samples

  1. 250ppb
    1. 2.53939 g of 985.5 ppb stock solutions
    2. DI Water added till final mass 10.01435g
    3. Actual Concentration: 249.898ppb
  2. 500ppb
    1. 5.08262 g of 985.5 ppb stock solutions
    2. DI Water added till final mass 10.0242g
    3. Actual Concentration: 499.822ppb
  3. 2ppm
    1. 0.21780 g of 96.5ppm standard
    2. water added to 10.00803g
    3. Actual Concentration: 2.1001ppm
  4. 4ppm
    1. 0.44046g of 96.5ppm standard
    2. water added to 10.02064g
    3. Actual Concentration: 4.2417ppm
  5. 6ppm
    1. 0.66000g of 96.5ppm standard
    2. water added to 10.03525g
    3. Actual Concentration: 6.3466ppm
  6. 8ppm
    1. 0.83007g of 96.5ppm standard
    2. water added to 10.01051
    3. Actual Concentration: 8.0018
  7. 10ppm
    1. 1.04895g of 96.5ppm standard
    2. water added to 10.02015g
    3. Actual Concentration: 10.1020ppm


ICP Parameters

Notes

This area is for any observations or conclusions that you would like to note.


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