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Elaine Marie Robbins/Notebook/MOF/2012/06/26
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MOF
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2012
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MMF Purification
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Methods
Dissolve MMF product in 30 mL chloroform.
Run through silica gel column with chloroform.
Rotovap.
Dissolve ~2.0 mg MMF product in 19 mL CH
3
CN at 75°C.
Slowly add 0.55 mL of 25.5 mM PdCl
2
(CH
3
CN)
2
in CH
3
CN.
Allow to sit at room temperature for 2 weeks.
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