User:Elaine Marie Robbins/Notebook/MOF/2012/06/01

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Methods

Filter PPF-4

  1. Pour PPF-4 onto Reeve Angel #802 filter paper on a watch glass.
  2. Allow to filter for 1 hr.
  3. Run powder XRD.


Synthesize PPF-18 and PPF-20 Cont.

  1. Slowly lower oven temperature to room temperature over the course of several hours.
  2. Pour PPF-18/20 onto Reeve Angel #802 filter paper on a watch glass.
  3. Allow to filter for 1 hr.

Data

  • XRD data of PPF-20 and PPF-4:
12-06-01 XRF of PPF20 and PPF4.png

Scan speeds: 0.5 deg/min for PPF-20 and PPF-4 (1), 0.2 deg/min for PPF-4 (2).

Sampling width: 0.010 degrees.