Difference between revisions of "User:Paul Rothenberg/Notebook/Pauls Notebook/2012/10/10"

From OpenWetWare
Jump to: navigation, search
(→‎10 October 2012)
(→‎10 October 2012)
Line 16: Line 16:
 
*Fluorescence revealed two peaks in the NiPPIX, at approximately 590 nm and 640 nm, indicating that there is a presence of porphyrin with no nickel and nickel porphyrin. The synthesis needs to be reperformed until the second peak is not present under fluorescence.  
 
*Fluorescence revealed two peaks in the NiPPIX, at approximately 590 nm and 640 nm, indicating that there is a presence of porphyrin with no nickel and nickel porphyrin. The synthesis needs to be reperformed until the second peak is not present under fluorescence.  
  
−
[Image:Absorbance of UV-Vis Graph.JPG]
+
[[Image:Absorbance of UV-Vis Graph.JPG]]
  
  

Revision as of 09:53, 10 October 2012

Owwnotebook icon.png Project name <html><img src="/images/9/94/Report.png" border="0" /></html> Main project page
<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>Previous entry<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>Next entry<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>

10 October 2012

  • 1. UV-Vis spectrum was calibrated with DMF. System checks were performed, and a baseline was run from 800-200 nm.
  • 2. DMF was used as a baseline, and run from 800-200 nm. The file was saved as a .spc file and a .txt file to dropbox
  • 3. DMF was then run under Fluorescence, and the file was saved to dropbox
  • 4. The 4μM NiPPIX was run under UV-VIS and Fluorescence
  • 5. The 2μM NIPPIX was run under UV-VIS and Fluorescence
  • 6. The 0.5μM NiPPIX was run under UV-VIS and Fluorescence
  • Fluorescence revealed two peaks in the NiPPIX, at approximately 590 nm and 640 nm, indicating that there is a presence of porphyrin with no nickel and nickel porphyrin. The synthesis needs to be reperformed until the second peak is not present under fluorescence.

Absorbance of UV-Vis Graph.JPG






Retrieved from "https://openwetware.org/mediawiki/index.php?title=User:Paul_Rothenberg/Notebook/Pauls_Notebook/2012/10/10&oldid=634410"