Difference between revisions of "User:Abigail E. Miller/Notebook/MOF Project/2013/02/05"

From OpenWetWare
Jump to: navigation, search
Line 24: Line 24:
  
 
==Data/Spectra==
 
==Data/Spectra==
* Insert content here...
+
* N/A
  
 
==Notes==
 
==Notes==
* Insert content here...
+
*  
  
 
<!-- ##### DO NOT edit below this line unless you know what you are doing. ##### -->
 
<!-- ##### DO NOT edit below this line unless you know what you are doing. ##### -->

Revision as of 14:31, 5 February 2013

Owwnotebook icon.png Metal Organic Frameworks <html><img src="/images/9/94/Report.png" border="0" /></html> Main project page
<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>Previous entry<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>

Objective

  • synthesis IRMOF's with adenine and guanine

Bench Work

  • need 500mg zinc nitrate hexahydrate (MW 297.5 g/mol), 154.3 mg Terephthalic acid (MW 166.13 g/mol) and either 63.5 mg guanine (MW 151.13 g/mol) or 56.8 mg adenine (MW 155.13 g/mol)
  • weighed out each component into a vial.
    • for IRMOF with guanine: 506.8 mg Zn(NO3)2 6H2O, 160 mg Terephthalic acid, 67 mg guanine
    • for IRMOF with adenine: 523.0 mg Zn(NO3)2 6H2O, 155 mg Terephthalic acid, 57.8 mg adenine
  • added approx 6 mL DMY to each vial
  • sonicated to dissolve leaving IRMOF-G vial with a white, opaque solution and the IFMOR-A vial with a clear transparent solution.
  • at 4pm place at 90 °C in a oven.


Data/Spectra

  • N/A

Notes