User:Elaine Marie Robbins/Notebook/MOF/2012/07/10

Synthesizing TBAPy	Main project page Previous entry      Next entry
Methods TBAPy Rotovap. Add enough water to dissolve solid. Mix at room temp for 2 hr. Adjust pH to 2 with concentrated HCl. Filter out solid. Wash with water, 1 M HCl, and diethyl ether. In2(OH)2(TBAPy) Mix 12 mg In(NO3)2•9H2O and 10 mg TBAPy in 4 mL DMF/dioxane/H2O (2/1/1). Add 10 μL of concentrated HCl. Heat at 85°C for 12 hr.