User
:
Elaine Marie Robbins/Notebook/MOF/2012/07/09
From OpenWetWare
<
User:Elaine Marie Robbins
|
Notebook
|
MOF
|
2012
|
07
Jump to navigation
Jump to search
Synthesizing TBAPy
Main project page
Previous entry
Next entry
Methods
Rotovap.
Recrystallize with hot toluene.
Filter out crystals with nylon filter paper.
Yield = 2.9799 g
Dissolve 1 g of solid in 100 mL THF/dioxane/H
2
O.
Add 20 mL of 2 M NaOH.
Stir under reflux at 85°C overnight.
Navigation menu
Page actions
User page
Talk
Read
View source
History
Page actions
User page
Talk
More
Tools
Personal tools
Log in
Request account
Navigation
Main Page
Recent changes
Help
Contact OWW
Add a Lab Notebook
Search
research
Materials
Protocols
Resources
Tools
What links here
Related changes
User contributions
Logs
View user groups
Special pages
Printable version
Permanent link
Page information