Objective
Description
Part 1: Crosslinking of 2 of the films prepared on 14/11/2012
Part 2: Prepare a film
- 1 ml of porphyrin (conc: 97.42micM)
Part 3: AA of the filtrates from 9/11/2012 & 14/11/2012
- The filtrates had to be diluted.
- 1 ml of each filtrate was mixed with 10 ml of HPLC water.
- Calculation(13 ppm of Cu ion was in the stick solution)
*M(1)*V(1)= M(2)*V(2)
*13ppm*1ml=M(2) *11ml
*M(2)=1.2 ppm
Data
AA results
- Actual concentration measured by AA of each filtrates are very close to each other except the number 2(gluteraldhyde filtrate of 30 min). (we stop the measurement too early therefore actual concentration of this filtrate should be ignored)
- AA results supports the UV-vis results from 14/11/1012.
Notes
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