User:Andrew W Long/Notebook/Synthesis of Lipid Modulators/2015/11/02

From OpenWetWare
Jump to: navigation, search
Owwnotebook icon.png Project name Report.pngMain project page
Resultset previous.pngPrevious entry      Next entryResultset next.png

Further purification of AL2

Today an MS of AL2 was run, and it was inconclusive (potentially the compound isn't very ionizable, because even though I put a considerable amount, the peaks for my compound did not predominate). Ross pointed out that I still had a strong peak at 73 (I think) which is DMF. I attempted to get rid of this by redissolving all of my compound in ethyl acetate, then running it under air for over a day.