User:Andrew K Farag/Notebook/CHEM-490/2014/10/20

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New procedure followed, combining the two last procedures used.

  • 5mL of 5mM HgNO3
  • 5mL BSA (15mg/mL)
  • both mixtures added in a 3-neck flask
  • final pH around 9 (adjusted by 1M NaOH)
  • temperature was set on 80C
  • two necks are covered with stopper
  • leave the flask in the hood under vacuum for 8-12 hours.