Uploads by Michael Wolfle
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This special page shows all uploaded files.
| Date | Name | Thumbnail | Size | Description |
|---|---|---|---|---|
| 20:37, 26 May 2011 | Pictet-Spengler cyclisation.png (file) |  |
21 KB | Bronsted-mediated Pictet-Spengler cyclisation of Ugi-intermediates of PZQ and derivatives |
| 19:08, 25 May 2011 | Ugi reaction.png (file) |  |
26 KB | Ugi-multicomponent reaction leading to PZQ intermediates |
| 18:40, 25 May 2011 | Isocyanides.png (file) |  |
18 KB | Synthesis isocyanides |
| 00:03, 25 May 2011 | BINOL-N-triflyl phosphoramide.png (file) |  |
21 KB | Synthesis (+/-)-BINOL-N-triflyl phosphoramide |
| 23:48, 24 May 2011 | N,N’-bis-3,5-bis(trifluoromethyl)phenyl-thiourea.png (file) | phenyl-thiourea.png){kind=small} |
12 KB | Synthesis of N,N’-bis[3,5-bis(trifluoromethyl)phenyl]thiourea |
| 23:33, 24 May 2011 | Binaphtyl-disulfonic acid procedure.gif (file) |  |
8 KB | Scheme: Synthesis 1,1-binaphthyl-2,2-disulfonic acid |
| 23:41, 17 May 2011 | Post-run Analysis.pdf (file) |  |
618 KB | Post-run processing and Shut-down |
| 23:37, 17 May 2011 | LCMS Notes-complete.pdf (file) | |
3.84 MB | Summary of all procedures |
| 23:27, 17 May 2011 | LCMS Starting Procedure.pdf (file) | |
958 KB | Starting Procedure to turn on the LCMS |
| 18:38, 17 May 2011 | New Method Creation.pdf (file) | |
2.58 MB | Creation of a new method for the Shimadzu LCMS |
| 18:33, 17 May 2011 | Batch setup and MS hardware.pdf (file) | |
855 KB | Description of the Shimadzu LC-MS hardware (ESI) and procedure to set up a batch sequence |
| 19:25, 16 February 2011 | Optical rotation as a function of the ee of R-PZQ.jpg (file) |  |
34 KB | Optical rotation [a] as a function of the ee of R-PZQ (EtOH, c=1) |
| 18:23, 16 February 2011 | Optical rotation as a function of the ee of S-PZQamine.jpg (file) |  |
34 KB | Optical rotation [a] as a function of the ee of S-PZQamine (DCM, c=1) |
| 22:37, 21 September 2010 | PZQamine.gif (file) |  |
5 KB | Hydrolysis of PZQ |
