Difference between revisions of "User:Paul Rothenberg/Notebook/Pauls Notebook/2013/06/12"

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(Reaction of OPD+H2O2 with Mb/PhosphateCatalyst in Acetone Suspension)
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==Reaction of OPD+H<sub>2</sub>O<sub>2</sub> with Mb/PhosphateCatalyst in Acetone Suspension==
 
==Reaction of OPD+H<sub>2</sub>O<sub>2</sub> with Mb/PhosphateCatalyst in Acetone Suspension==
  
We are going to run the same reaction as yesterday, but, the samples will be centrifuged before a spectrum is taken. Hopefully, the results will be more consistent than yesterday's. We will not filter the solution; just remove a 1 mL sample and take a spectrum of it.
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We are going to run the same reaction as yesterday, but, the samples will be centrifuged before a spectrum is taken. Hopefully, the results will be more consistent than yesterday's.  
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We let the reaction run for 20 minute intervals, took a 1 mL sample, and centrifuged it for 1 minute at 13,200 rpm.  
  
 
<b>Data:</b>
 
<b>Data:</b>
  
[[Image:Mb_Phosphate_OPD_H2O2_Acetone_RERUN_GRAPH.png]]
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[[Image:Mb_Phosphate_OPD_H2O2_Acetone_RERUN_GRAPH.png|750px]]
  
 
==Reaction of OPD+H<sub>2</sub>O<sub>2</sub> with Mb/Acetate Catalyst in Acetone Suspension==
 
==Reaction of OPD+H<sub>2</sub>O<sub>2</sub> with Mb/Acetate Catalyst in Acetone Suspension==
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[[Image:Mb_Acetate_OPD_H2O2_Acetone_RERUN_WORKUP_GRAPH.png|750px]]
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==Reaction of OPD+H<sub>2</sub>O<sub>2</sub> with Mb/Citrate Catalyst in Acetone Suspension==
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[[Image:Mb_Citrate_OPD_H2O2_Acetone_WORKUP_GRAPH.png|750px]]
 
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Reaction of OPD+H2O2 with Mb/PhosphateCatalyst in Acetone Suspension

We are going to run the same reaction as yesterday, but, the samples will be centrifuged before a spectrum is taken. Hopefully, the results will be more consistent than yesterday's.


We let the reaction run for 20 minute intervals, took a 1 mL sample, and centrifuged it for 1 minute at 13,200 rpm.

Data:

Mb Phosphate OPD H2O2 Acetone RERUN GRAPH.png

Reaction of OPD+H2O2 with Mb/Acetate Catalyst in Acetone Suspension

Mb Acetate OPD H2O2 Acetone RERUN WORKUP GRAPH.png


Reaction of OPD+H2O2 with Mb/Citrate Catalyst in Acetone Suspension

Mb Citrate OPD H2O2 Acetone WORKUP GRAPH.png