User:Matthew R Skorski/Notebook/Cellulose Summer 2014/2014/06/13

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Entry title Purpose: To run XRD and DSC of old samples Safety and Procedure: For XRD machine the samples were run on attachment 2 and condition 2. For the DSC the samples were sealed using hermetic cap and lids. The parameters of this run are listed below 1: Ramp 40.00 °C/min to 170.00 °C 2: Isothermal for 2.00 min 3: Ramp 40.00 °C/min to 110.00 °C 4: Isothermal for 60.00 min 5: Ramp 40.00 °C/min to 20.00 °C 6: Isothermal for 2.00 min 7: Mark end of cycle 0 8: Ramp 10.00 °C/min to 170.00 °C 9: Isothermal for 2.00 min 10: Ramp 10.00 °C/min to 20.00 °C The reference pan and number used were the ones listed on the machine. Experimental: XRD 5/20/2014 NH4+-CNC in ABS 1% 5/20/2014 NH4+-CNC in ABS 5% 5/20/2014 NH4+-CNC in ABS 10% 5/20/2014 NH4+-CNC in ABS 20% 6/2/14 NH4+-CNC in ABS 25% 6/2/14 TiO2 in PLA 30% 6/2/14 TiO2 in PLA 40% 6/2/14 TiO2 in PLA 50% 5/5/2014 Straight NH4+-CNC powder DSC 5/20/2014 NH4+-CNC in ABS Mass% Mass Pan + Lid Mass Sample 1% 52.40 mg 3.17 mg 5% 52.42 mg 3.15 mg 10% 52.66 mg 2.86 mg 20% 52.27 mg 3.09 mg 6/9/14 NH4+-CNC in ABS Mass% Mass Pan + Lid Mass Sample 20% #2 52.29 mg 3.04 mg 10% #2 52.84 mg 3.07 mg