User:Andrew W Long/Notebook/Synthesis of Lipid Modulators/2015/11/02

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Further purification of AL2

Today an MS of AL2 was run, and it was inconclusive (potentially the compound isn't very ionizable, because even though I put a considerable amount, the peaks for my compound did not predominate). Ross pointed out that I still had a strong peak at 73 (I think) which is DMF. I attempted to get rid of this by redissolving all of my compound in ethyl acetate, then running it under air for over a day.



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