User:Moira M. Esson/Notebook/CHEM-581/2013/02/06: Difference between revisions
From OpenWetWare
Line 89: | Line 89: | ||
*After allowing the clays to spin for 4 days, the prepared clays were vacuum filtered following the protocol described on [[User:Moira_M._Esson/Notebook/CHEM-581/2012/09/19|2012/09/19]]. | *After allowing the clays to spin for 4 days, the prepared clays were vacuum filtered following the protocol described on [[User:Moira_M._Esson/Notebook/CHEM-581/2012/09/19|2012/09/19]]. | ||
*For the 110% exchanged clays, after 4 hours on the vacuum filter, the clays were not dry. In order to have complete drying of the clays, the remaining wet clay was scraped from the Buchner funnel, placed on a tin tray, and placed in an oven at 90°C. | *For the 110% exchanged clays, after 4 hours on the vacuum filter, the clays were not dry. In order to have complete drying of the clays, the remaining wet clay was scraped from the Buchner funnel, placed on a tin tray, and placed in an oven at 90°C. | ||
==DSC== | |||
{| {{table}} | |||
| align="center" style="background:#f0f0f0;"|'''DSC sample preparation''' | |||
| align="center" style="background:#f0f0f0;"|'''''' | |||
| align="center" style="background:#f0f0f0;"|'''''' | |||
|- | |||
| Name of sample||Mass of pan(g)||Mass of sample(g) | |||
|- | |||
| NaMT clay||0.04813||0.00316 | |||
|- | |||
| Lamp clay||0.05018||0.00306 | |||
|- | |||
| 110% Lamp exchange||0.04952||0.00308 | |||
|- | |||
| 110% NaMT exchange||0.05014||0.00301 | |||
|- | |||
| 50% NaMT exchange||0.04819||0.0029 | |||
|} | |||
*The prepared samples will be run the next time in the lab. | |||
Revision as of 12:14, 7 February 2013
Project name | <html><img src="/images/9/94/Report.png" border="0" /></html> Main project page <html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>Previous entry<html> </html>Next entry<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html> | |||||||||||||||||||||||||||||||||
Objectives
PVA MicrospheresGeneral Protocol:
Hydrogel Preparation
Clay Filtration
DSC
|