User:Michael S. Bible/Notebook/Summer MOF Research/2016/07/22: Difference between revisions

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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span>
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|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
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==Entry title==
==Create DSC Samples==
* Insert content here...
* DSC samples were prepared from the 10% MOF-5, 10% HKUST-1, 10% ZIF-8, 50% MOF-5, and ABS filaments.  
* Each sample consists of the following masses:
* '''10% MOF-5''': Sample Mass - 2.96 mg, DSC Pan mass - 39.99 mg
* '''10% ZIF-8''': Sample Mass - 3.13 mg, DSC Pan mass - 40.09 mg
* '''10% HKUST-1''': Sample Mass - 3.27 mg, DSC Pan mass - 40.02 mg
* '''50% MOF-5''': Sample Mass - 2.89 mg, DSC Pan mass - 40.17 mg
* '''ABS''': Sample Mass - 3.23 mg, DSC Pan mass - 39.01 mg


==Create PXRD Samples==
* PXRD samples were created from the 50% MOF-5 in ABS filament and 10% HKUST-1 in ABS filament. 
* About 1.05g of each was pressed at 195 °C
* The discs were removed and still had very noticeable grain boundaries, so they were re-pressed at 220°C
* Despite the increased temperature, the materials still did not appear homogeneous.  It was determined, however, that this would be sufficient for PXRD. 


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Latest revision as of 01:50, 27 September 2017

Project name Main project page
Previous entry      Next entry

Create DSC Samples

  • DSC samples were prepared from the 10% MOF-5, 10% HKUST-1, 10% ZIF-8, 50% MOF-5, and ABS filaments.
  • Each sample consists of the following masses:
  • 10% MOF-5: Sample Mass - 2.96 mg, DSC Pan mass - 39.99 mg
  • 10% ZIF-8: Sample Mass - 3.13 mg, DSC Pan mass - 40.09 mg
  • 10% HKUST-1: Sample Mass - 3.27 mg, DSC Pan mass - 40.02 mg
  • 50% MOF-5: Sample Mass - 2.89 mg, DSC Pan mass - 40.17 mg
  • ABS: Sample Mass - 3.23 mg, DSC Pan mass - 39.01 mg

Create PXRD Samples

  • PXRD samples were created from the 50% MOF-5 in ABS filament and 10% HKUST-1 in ABS filament.
  • About 1.05g of each was pressed at 195 °C
  • The discs were removed and still had very noticeable grain boundaries, so they were re-pressed at 220°C
  • Despite the increased temperature, the materials still did not appear homogeneous. It was determined, however, that this would be sufficient for PXRD.


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