User:Mary Mendoza/Notebook/CHEM 581: Experimental Chemistry I/2014/09/10: Difference between revisions
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==Cross-linking and Neutralizing Batch 4 Films== | ==Cross-linking and Neutralizing Batch 4 Films== | ||
* | * Film synthesis was completed using the protocol from [[User:Matt Hartings/Notebook/AU Biomaterials Design Lab/2014/08/29|August 29, 2014.]] | ||
==Film Synthesis with Ion Exchange using Ionic Liquids== | ==Film Synthesis with Ion Exchange using Ionic Liquids== | ||
* Using the information from [[User:Matt Hartings/Notebook/AU Biomaterials Design Lab/2014/09/10|Dr. Hartings' entry]], [[User:James C. Schwabacher/Notebook/CHEM-571/2014/09/10|James]] performed the following procedure to initiate the organic cation exchange: | |||
**1.1046 g of Sodium Montmorillonite was added to a vial | |||
**Assuming 92 meq of Na per 100 g, the total eq was 10.16232E-04 | |||
**Added 0.5251 g tributylhexadecylphosphonium bromide (MW=507.65) to the vial | |||
**Added 10 mL of HPLC water and 10 mL ethanol | |||
**capped the vial and set to stir for one week | |||
==Preparation of Film Sample for Powder X-RAY Diffraction== | ==Preparation of Film Sample for Powder X-RAY Diffraction== |
Revision as of 12:16, 19 September 2014
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Cross-linking and Neutralizing Batch 4 Films
Film Synthesis with Ion Exchange using Ionic Liquids
Preparation of Film Sample for Powder X-RAY Diffraction
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