User:Mary Mendoza/Notebook/CHEM 581: Experimental Chemistry I/2014/09/10: Difference between revisions
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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span> | |style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span> | ||
|style="background-color: #F2F2F2" align="center"| | |style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]] }}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}} | ||
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==Cross-linking and Neutralizing Batch 4 Films== | ==Cross-linking and Neutralizing Batch 4 Films== | ||
* | * Film synthesis was completed using the protocol from [[User:Matt Hartings/Notebook/AU Biomaterials Design Lab/2014/08/29|August 29, 2014.]] | ||
==Film Synthesis with Ion Exchange using Ionic Liquids== | ==Film Synthesis with Ion Exchange using Ionic Liquids== | ||
* Using the information from [[User:Matt Hartings/Notebook/AU Biomaterials Design Lab/2014/09/10|Dr. Hartings' entry]], [[User:James C. Schwabacher/Notebook/CHEM-571/2014/09/10|James]] performed the following procedure to initiate the organic cation exchange: | |||
**1.1046 g of Sodium Montmorillonite was added to a vial | |||
**Assuming 92 meq of Na per 100 g, the total eq was 10.16232E-04 | |||
**Added 0.5251 g tributylhexadecylphosphonium bromide (MW=507.65) to the vial | |||
**Added 10 mL of HPLC water and 10 mL ethanol | |||
**capped the vial and set to stir for one week | |||
==Preparation of Film Sample for Powder X-RAY Diffraction== | ==Preparation of Film Sample for Powder X-RAY Diffraction== | ||
* Incised a PVA-clay film with the size of the scintillating vial lid. | * Incised a PVA-clay film with the size of the scintillating vial lid. | ||
* The film was suspended in 10 mL of 2ppm MG solution contained in a scintillating vial. The MG solution for this sample was prepared from | * The film was suspended in 10 mL of 2ppm MG solution contained in a scintillating vial. The MG solution for this sample was prepared from the stock solution prepared on [[User:James C. Schwabacher/Notebook/CHEM-571/2014/08/29|August 29, 2014.]] | ||
* The sample will be analyzed for the following lab meeting on September 12, 2014. | * The sample will be analyzed for the following lab meeting on September 12, 2014. | ||
Latest revision as of 00:16, 27 September 2017
Project name | Main project page Previous entry Next entry |
Cross-linking and Neutralizing Batch 4 Films
Film Synthesis with Ion Exchange using Ionic Liquids
Preparation of Film Sample for Powder X-RAY Diffraction
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