User:James C. Schwabacher/Notebook/CHEM-571/2014/09/12: Difference between revisions
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|style="background-color: #EEE"|[[Image:BDLlogo_notext_lr.png|128px]]<span style="font-size:22px;"> Biomaterials Design Lab</span> | |style="background-color: #EEE"|[[Image:BDLlogo_notext_lr.png|128px]]<span style="font-size:22px;"> Biomaterials Design Lab</span> | ||
|style="background-color: #F2F2F2" align="center"| | |style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]] }}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}} | ||
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==Objective== | ==Objective== | ||
*Preparation of 10% NaMT exfoliated materials | |||
*Perform pXRD measurements | |||
*Analyze DSC and UVVis data | |||
==Description== | ==Description== | ||
# | # Exfoliated Clays | ||
## 2.7756 g of 4% NaMT "sludge" was weighed out with 0.9996 g of PVA to synthesize the exfoliated film following the original protocol | |||
# pXRD | |||
## Samples were blotted dry with Kimwipes before being taped down the pXRD discs | |||
#New Malachite Green/PVA Film experiments | |||
## 200 ppm stock solution prepared by [[User:Madeleine_Y._Bee/Notebook/CHEM-581_Experimental_Chemistry/2014/09/12|Madeleine and Alicia]] | |||
## 80 ppm solution prepared by [[User:Eleni_N._Kalivas/Notebook/CHEM-571/2014/09/12|Eleni and Melvin]] | |||
## 8 ppm solution prepared by [[User:Andrew_K_Farag/Notebook/CHEM-581/2014/09/12|Andrew, Tami and Michael]] | |||
## 2 ppm stock solution was prepared using 1 ml of the 200 ppm stock solution and water in a 100 mL volumetric flask | |||
## Samples of PVA film were cut and massed | |||
## 10 ml of each solution were placed in separate vials with film samples | |||
## 2 ppm and 200 ppm malachite green solution controls were taken by placing 10 ml of each in empty vials | |||
### [[User:Madeleine_Y._Bee/Notebook/CHEM-581_Experimental_Chemistry/2014/09/12|Madeleine and Alicia]] prepared 80 ppm and 200 ppm control samples | |||
### [[User:Andrew_K_Farag/Notebook/CHEM-581/2014/09/12|Andrew, Tami and Michael]] prepared 8 ppm and 80 ppm control samples | |||
### [[User:Eleni_N._Kalivas/Notebook/CHEM-571/2014/09/12|Eleni, Melvin and Becky]] prepared 2 ppm and 8 ppm control samples | |||
==Data== | ==Data== | ||
* | * PVA Film + Malachite Green Solution mass data: [[Image:PVA_Film_Table_of_Values_-_MJJ.png]] | ||
==Notes== | ==Notes== |
Latest revision as of 00:16, 27 September 2017
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Objective
Description
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