User:Ellen Petersen/Notebook/MOF/2012/04/12: Difference between revisions
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== | ==DPNI Take 1== | ||
* | * 1.) 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.805g, 3.00 mmol) | ||
*2.) 4- aminopyridine (.847 g, 6.00 mmol) | |||
*3.) Diethyl ether (600 mL | |||
*4.) Dimethylacetamide (DMA) (150 mL) | |||
Dissolve 1&2 in DMA stirred at 135 degrees C overnight | |||
cooled to room temperature and poured onto diethyl ether (600 mL) | |||
precipitate filter and washed with diethyl ether | |||
dried under vacuum to yield | |||
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DPNI Take 1
Dissolve 1&2 in DMA stirred at 135 degrees C overnight cooled to room temperature and poured onto diethyl ether (600 mL) precipitate filter and washed with diethyl ether dried under vacuum to yield
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