User:Ellen Petersen/Notebook/MOF/2012/04/12: Difference between revisions
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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> | |style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> MOF</span> | ||
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html> </html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}} | |style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html> </html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}} | ||
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==DPNI | ==DPNI: 04-12-12== | ||
* 1.) 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.805g, 3.00 mmol) | * 1.) 1,4,5,8 Naphthalenetetracarboxylic dianhydride (.805g, 3.00 mmol) | ||
*2.) 4- aminopyridine (.847 g, 6.00 mmol) | *2.) 4- aminopyridine (.847 g, 6.00 mmol) | ||
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*4.) Dimethylacetamide (DMA) (150 mL) | *4.) Dimethylacetamide (DMA) (150 mL) | ||
Dissolve 1&2 in DMA stirred at 135 degrees C overnight | *5.) Dissolve 1&2 in DMA stirred at 135 degrees C overnight. | ||
*6.) Cooled to room temperature and poured onto diethyl ether (600 mL). | |||
*7.) Precipitate filter and washed with diethyl ether | |||
dried under vacuum to yield | *8.) dried under vacuum to yield | ||
Revision as of 08:43, 28 June 2013
MOF | <html><img src="/images/9/94/Report.png" border="0" /></html> Main project page Next entry<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html> |
DPNI: 04-12-12
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