User:Andrew W Long/Notebook/Synthesis of Lipid Modulators/2015/10/02: Difference between revisions
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Procedure for large-scale rxn: | Procedure for large-scale rxn: | ||
#Calculations: | #Calculations: | ||
##<math>\frac{ | ##Get moles of 2-chloro <math>\frac{250mg}{1}|\frac{1g}{1000mg}|\frac{1mol}{158.54g}=0.00158mol</math> | ||
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Revision as of 16:00, 5 October 2015
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Purification of Product of Rxn Between MTT and CNP, and Large-Scale Reaction SetupNote that MTT refers to 5-(methylthio)-1,3,4-thiadiazole-2-thiol, and that CNP refers to 2-chloro-3-nitropyridine. Structures shown here Goals:
Procedure for purification:
Procedure for large-scale rxn:
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