User:Andrew W Long/Notebook/Synthesis of Lipid Modulators/2015/10/02: Difference between revisions

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==Purification of Product of Rxn Between MTT and CNP==
==Purification of Product of Rxn Between MTT and CNP==
*Note that MTT refers to 5-(methylthio)-1,3,4-thiadiazole-2-thiol, and that CNP refers to 2-chloro-3-nitropyridine. Structures shown [[User:Andrew_W_Long/Notebook/Synthesis_of_Lipid_Modulators/2015/09/21#Reaction_of_5-.28methylthio.29-1.2C3.2C4-thiadiazole-2-thiol_.26_2-chloro-3-nitropyridine|here]]
*Note that '''MTT''' refers to 5-(methylthio)-1,3,4-thiadiazole-2-thiol, and that '''CNP''' refers to 2-chloro-3-nitropyridine. Structures shown [[User:Andrew_W_Long/Notebook/Synthesis_of_Lipid_Modulators/2015/09/21#Reaction_of_5-.28methylthio.29-1.2C3.2C4-thiadiazole-2-thiol_.26_2-chloro-3-nitropyridine|here]]
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Procedure:





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Purification of Product of Rxn Between MTT and CNP

  • Note that MTT refers to 5-(methylthio)-1,3,4-thiadiazole-2-thiol, and that CNP refers to 2-chloro-3-nitropyridine. Structures shown here

Procedure: