User:Paul Rothenberg/Notebook/Pauls Notebook/2013/06/27

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Reaction of OPD+H2O2 in H2O with Mb/Citrate Catalyst

Dhea and I are going back to running this reaction as a kinetics reaction. We are going back to the way I began running these, by dissolving everything in the solvent and running the reactions at temperature for 10 minutes. For the full workup procedure, refer to May 20.

Data:

Mb Citrate OPD H2O2 H2O 5 GRAPH Trial2.png

Mb Citrate OPD H2O2 H2O 5C SEQUENTIAL GRAPH Trial2.png

Mb Citrate OPD H2O2 H2O 15 GRAPH Trial2.png

Mb Citrate OPD H2O2 H2O 15C SEQUENTIAL GRAPH Trial2.png The baseline was off here, leaving odd results. The reaction still proceeded forwards, but it is not fully evident based on the graph.

Mb Citrate OPD H2O2 H2O 25 GRAPH Trial2.png

Mb Citrate OPD H2O2 H2O 25C SEQUENTIAL GRAPH Trial2.png

Mb Citrate OPD H2O2 H2O 35 GRAPH Trial2.png

Mb Citrate OPD H2O2 H2O 35C SEQUENTIAL GRAPH Trial2.png

Mb Citrate OPD H2O2 H2O 45 GRAPH Trial2.png

Mb Citrate OPD H2O2 H2O 55 GRAPH Trial2.png

Mb Citrate OPD H2O2 H2O 55 SEQUENTIAL GRAPH Trial2.png

Mb Citrate OPD H2O2 H2O 65 GRAPH Trial2.png

Mb Citrate OPD H2O2 H2O 65C SEQUENTIAL GRAPH Trial2.png

Trial 3 Data:

Mb Citrate OPD H2O2 H2O 5C GRAPH Trial3.png

Mb Citrate OPD H2O2 H2O 5C SEQUENTIAL GRAPH Trial3.png

Mb Citrate OPD H2O2 H2O 15C GRAPH Trial3.png

Mb Citrate OPD H2O2 H2O 15C SEQUENTIAL GRAPH Trial3.png

Mb Citrate OPD H2O2 H2O 25C GRAPH Trial3.png

Mb Citrate OPD H2O2 H2O 25C SEQUENTIAL GRAPH Trial3.png

Mb Citrate OPD H2O2 H2O 35C GRAPH Trial3.png

Mb Citrate OPD H2O2 H2O 35C SEQUENTIAL GRAPH Trial3.png

Mb Citrate OPD H2O2 H2O 45C GRAPH Trial3.png

Mb Citrate OPD H2O2 H2O 45C SEQUENTIAL GRAPH Trial3.png

Mb Citrate OPD H2O2 H2O 55C GRAPH Trial3.png

Mb Citrate OPD H2O2 H2O 55C SEQUENTIAL GRAPH Trial3.png