User:Paul Rothenberg/Notebook/Pauls Notebook/2013/06/10

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Reaction of OPD+H2O2 with Mb/Citrate Catalyst in Acetonitrile Suspension

Instead of running this reaction in the previous fashion, we are going to try to run this in a beaker with a stir bar to prevent the reaction tube to be shaken every few minutes. We will also filter the solution before taking a spectrum. We will follow the same procedure as with the Isopropanol suspension and the previous acetonitrile suspensions.

10:05: The reaction was started. Samples were removed every 20 minutes and pushed through a syringe filter directly into the cuvette. 7 samples total were taken and analyzed.

Data:

Mb Citrate OPD H2O2 MeCN FILTERED WORKUP GRAPH.png


Reaction of OPD+H2O2 with Mb/Phosphate Catalyst in Acetonitrile Suspension

Data:

Mb Phosphate OPD H2O2 MeCN FILTERED WORKUP GRAPH.png

Reaction of OPD+H2O2 with Mb/Acetate Catalyst in Acetonitrile Suspension

Data:

Mb Acetate OPD H2O2 MeCN FILTERED WORKUP GRAPH.png