User:Matthew R Skorski/Notebook/Cellulose Summer 2014/2014/06/13

From OpenWetWare
Jump to: navigation, search
Owwnotebook icon.png Project name Report.pngMain project page
Resultset previous.pngPrevious entry      Next entryResultset next.png

Entry title

Purpose: To run XRD and DSC of old samples

Safety and Procedure: For XRD machine the samples were run on attachment 2 and condition 2. For the DSC the samples were sealed using hermetic cap and lids. The parameters of this run are listed below

  • 1: Ramp 40.00 °C/min to 170.00 °C
  • 2: Isothermal for 2.00 min
  • 3: Ramp 40.00 °C/min to 110.00 °C
  • 4: Isothermal for 60.00 min
  • 5: Ramp 40.00 °C/min to 20.00 °C
  • 6: Isothermal for 2.00 min
  • 7: Mark end of cycle 0
  • 8: Ramp 10.00 °C/min to 170.00 °C
  • 9: Isothermal for 2.00 min
  • 10: Ramp 10.00 °C/min to 20.00 °C

The reference pan and number used were the ones listed on the machine.

Experimental:

XRD

  • 5/20/2014 NH4+-CNC in ABS 1%
  • 5/20/2014 NH4+-CNC in ABS 5%
  • 5/20/2014 NH4+-CNC in ABS 10%
  • 5/20/2014 NH4+-CNC in ABS 20%
  • 6/2/14 NH4+-CNC in ABS 25%
  • 6/2/14 TiO2 in PLA 30%
  • 6/2/14 TiO2 in PLA 40%
  • 6/2/14 TiO2 in PLA 50%
  • 5/5/2014 Straight NH4+-CNC powder

DSC

5/20/2014 NH4+-CNC in ABS

 Mass%   Mass Pan + Lid   Mass Sample
 1%      52.40 mg         3.17 mg
 5%      52.42 mg         3.15 mg
 10%     52.66 mg         2.86 mg
 20%     52.27 mg         3.09 mg

6/9/14 NH4+-CNC in ABS

Mass%    Mass Pan + Lid   Mass Sample
20% #2   52.29 mg         3.04 mg
10% #2   52.84 mg         3.07 mg