User:Jerinbrooks/Notebook/JB:481:18/2018/09/07

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Objective

  1. Use a calibration standard solution to take the ICP of diluted samples of standard solution

Description

  1. Dilutions of (100 μg/mL)(1 mL/1.036) of Density:1.036g/mL standard were made
  2. Starting conditions of ICP were set
  3. Between each sample ICP tubed was rinsed with HPLC water
  • Starting conditions

ICP-Para1.JPG

ICP-Para2.JPG

ICP-Para3.JPG

Data

  1. Newly made solutions
    1. [1.036g of 96.5ppm sample used, add water for total of 10.016]=10.26ppm
    2. [0.8288g of 96.5ppm standard, add water for total 10.001g]=7.96ppm
    3. [0.6216g of 96.5ppm standard, add water for total 10.035]=6.12ppm
    4. [0.4144g of 96.5ppm standard, add water for total 10.202g]=4.058ppm
    5. [0.2072g of 96.5ppm standard, add water for total 10.057g]=2.22ppm
    6. [0.1036g of 96.5ppm standard, add water for total 50.02g]=1.038ppm
    7. [4.816g of 1.038ppm standard, add water for total 10.002g]=0.5011ppm
    8. [2.408g of 1.038ppm standard, add water for total 10.008g]=0.2491ppm


Notes