User:James C. Schwabacher/Notebook/CHEM-571/2014/09/17

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Objective

  • MG measurements from PVA trial 2
  • Continue film synthesis from last week
  • Filter
  • Begin pXRD measurement
  • Finish compiling DSC data

Description

  1. Data collection from the DSC was completed
    1. a table of values and graphs of the temperature vs. heat flow can be seen below
  2. UV-Vis of the MG PVA films
    1. the data previously collected from the absorption of the PVA only films seemed off when compared to values with the class.
    2. New films were produced, allowed to absorb concentrations of Malachite Green, and UV-Vis was run on the different concentrations.
    3. Information on the new experiment can be viewed here.
  3. Ionic Liquid Exchange
  4. Started the XRD of the MG PVA-Clay Films
    1. Dr. Hartings produced the clay control in slot 1
      1. Madeleine's group produced the 8ppm sample in slot 2
      2. My group produced the 2ppm sample in slot 3
      3. My group produced the PVA film control in slot 4
      4. Eleni's group produced the 80ppm sample in slot 5
      5. Tami's group produced the 200ppm sample in slot 6
  5. Finished exfoliated clay film
    1. The procedure followed the standard film synthesis. This may be viewed here.

Data: DSC Table

PVA Conc. (ppm) ' Energy (J/g) H₂0 (mg) Glass Transition (⁰C) Water Evaporation Peak (⁰C)
2 928.4 1.3239 69.11 and 79.8 108.58
8 1001 1.9796 68.77 99.31
80 1340 2.9384 68.338 105.91
200 819.4 1.0803 68.63 128.77
Control 582.9 0.95407 68.566 125.61
PVA-Clay 2 1303 1.8931 68.716 100.97
8 883.8 1.4585 68.644 99.59
80 861.3 2.2633 68.866 102.05, 106.55, and 128.44
200 N/A N/A N/A N/A
Control 671.2 0.90296 69.164 116.15 and 105.16

Data: PVA only DSC Graphs

DSC PVA CONTROL MG MJJ 092014.png DSC PVA 2ppm MG MJJ 092014.png DSC PVA 8ppm MG MJJ 092014.png DSC PVA 80ppm MG MJJ 092014.png DSC PVA 200ppm MG MJJ 092014.png

Data: PVA + NaMT DSC Graphs

DSC PVA NaMT CONTROL MG MJJ 092014.png DSC PVA NaMT 2ppm MG MJJ 092014.png DSC PVA NaMT 8ppm MG MJJ 092014.png DSC PVA NaMT 80ppm MG MJJ 092014.png DSC PVA NaMT 200ppm MG MJJ 092014.png DSC PVA NaMT 200ppm zoomed MG MJJ 092014.png