- Make a batch (A)
- Start DSC and FTIR
- of ABS beads, 1%, 5%, 10%
- Batch A
- 50.036g of ABS beads were added to 500mL of Acetone
- Mixture was sonicated at 69°C for 225 minutes
- Tzero pans and hermetic lids were weighed and a ≈5mg sample was added. Actual values may be viewed on the table below.
- Samples were either an ABS bead or 1%, 5%, 10% TiO2 ABS filament
- The runs followed the following procedure:
- Jump to 20°C
- Isothermal at 20°C for 2 min
- Ramp 5°C/min until 140°C
- Isothermal at 140°C for 2 min
- Ramp 5°C/min until 110°C
- Isothermal at 110°C for 10 min
- Ramp 5°C/min until 20°C
- Repeat cycle 2 times
| ABS Bead
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