User
:
Elaine Marie Robbins/Notebook/MOF/2012/07/24
From OpenWetWare
<
User:Elaine Marie Robbins
|
Notebook
|
MOF
|
2012
|
07
Jump to navigation
Jump to search
PPF-18
Main project page
Previous entry
Next entry
Methods
Filter In
2
(OH)
2
TBAPy.
Wash In
2
(OH)
2
TBAPy with DMF.
Collect crystals.
Run powder XRD.
Use Rh 6G in EtOH to perform FRET.
Synthesize PPF-18.
Mix 7.9 mg TCPP, 8.9 mg Zn(NO
3
)
2
•6H
2
O, and 4.2 mg DPNI.
Add 50 μL 1.0 M acidic EtOH.
Add 1.5 mL DEF and 0.5 mL EtOH.
Sonicate.
Heat to 80°C for 24 hr.
Data
Powder XRD of three batches of In
2
(OH)
2
TBAPy:
Fluorescence of In
2
(OH)
2
TBAPy and rhodamine 6G, excited at 200 nm:
Navigation menu
Page actions
User page
Talk
Read
View source
History
Page actions
User page
Talk
More
Tools
Personal tools
Log in
Request account
Navigation
Main Page
Recent changes
Help
Contact OWW
Add a Lab Notebook
Search
research
Materials
Protocols
Resources
Tools
What links here
Related changes
User contributions
Logs
View user groups
Special pages
Printable version
Permanent link
Page information