User:Elaine Marie Robbins/Notebook/MOF/2012/07/13

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Owwnotebook icon.png PPF-20 with DNA Bases Report.pngMain project page
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Methods

  1. Synthesize PPF-20 solutions with adenine/guanine linkers.
    1. Slowly cool.
    2. Filter with nylon filter paper.
    3. Run powder XRD.
  2. Make more PPF-20 (with DPNI linkers)
    1. Mix 7.9 mg TCPP, 8.9 mg Zn(NO3)2•6H2O, 16.8 mg DPNI, and 30 μL 1.0 M acidic EtOH.
    2. Add 1.5 mL DMF and 0.5 mL EtOH.
    3. Sonicate.
    4. Heat at 85°C for 24 hr.
  3. Synthesize In2(OH)2TBAPy.
    1. Mix 12 mg In(NO3)3•9H2O and 10 mg TBAPy in 4 mL DMF/dioxane/H2O (2/1/1).
    2. Add 10 μL concentrated HCl.
    3. Heat at 85°C for 12 hours.