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Elaine Marie Robbins/Notebook/MOF/2012/07/12
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2012
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Methods
Synthesize PPF-20 using purines instead of DPNI.
Mix 7.9 mg TCPP, 8.9 mg Zn(NO
3
)
2
•6H
2
O, 16.8 mg of a purine, and 30 μL of 1.0 M acidic EtOH.
Purines used: adenine, guanine.
Add 0.5 mL EtOH and 1.5 mL DMF.
Sonicate.
Heat at 80°C for 24 hr.
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