User:Elaine Marie Robbins/Notebook/MOF/2012/07/12

From OpenWetWare
Jump to navigationJump to search
Purine Linkers Main project page
Previous entry      Next entry

Methods

  1. Synthesize PPF-20 using purines instead of DPNI.
    1. Mix 7.9 mg TCPP, 8.9 mg Zn(NO3)2•6H2O, 16.8 mg of a purine, and 30 μL of 1.0 M acidic EtOH.
      • Purines used: adenine, guanine.
    2. Add 0.5 mL EtOH and 1.5 mL DMF.
    3. Sonicate.
    4. Heat at 80°C for 24 hr.