User:Elaine Marie Robbins/Notebook/MOF/2012/07/10

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Methods

TBAPy

  1. Rotovap.
  2. Add enough water to dissolve solid.
  3. Mix at room temp for 2 hr.
  4. Adjust pH to 2 with concentrated HCl.
  5. Filter out solid.
  6. Wash with water, 1 M HCl, and diethyl ether.


In2(OH)2(TBAPy)

  1. Mix 12 mg In(NO3)2•9H2O and 10 mg TBAPy in 4 mL DMF/dioxane/H2O (2/1/1).
  2. Add 10 μL of concentrated HCl.
  3. Heat at 85°C for 12 hr.