User:Elaine Marie Robbins/Notebook/MOF/2012/07/05

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  1. Rotovap.
  2. Add enough water to dissolve solid.
  3. Stir for 2 hr.
  4. Adjust pH to 2 with HCl.
  5. Filter out solid.
  6. Wash crystals with water, HCl, and diethyl ether.