User:Elaine Marie Robbins/Notebook/MOF/2012/06/20

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  1. Bubble N2 through 14 mL of THF for 30 min.
  2. Add 1.04 g of o-phenylenediamine and 1.30 g of terephthalaldehyde.
  3. Heat at 50°C for 26 hr in a reflux column under N2.