User:Dhea Patel/Notebook/Phosphorylation/2012/03/29

Phosphorylation Lab

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Objective Learn how to maintain an OpenWetWare Notebook. Preparing [Ru(bpy)2(phen-IA)](PF6)2 Calculations were made to determine how much (1,10)-Phenanthrolin-5-amine to use in this experiment. 500 mg of 0.0961 mmol Ru(bpy)2Cl2 and 207mg of 1.06 mmol (1,10)-Phenanthrolin-5-amine were refluxed in 25mL MeOH for about 3 hours with stirring. The solution changed from a dark purple to a orange-red during the reflux. Calculating Mass of (1,10)-Phenanthrolin-5-amine 1000 mmol = 1 mol 195.22g/mol ÷ 1000mmol/mol = 0.19522 g/mmol 1.06mmol × 0.19522 g/mmol = 0.207 g or 207 mg Data Add data and results here... Notes This area is for any observations or conclusions that you would like to note.