User:Dhea Patel/Notebook/Hemoglobin Project/2013/06/11

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Reaction of OPD+H2O2 with Mb Catalyst in Acetonitrile Suspension

The procedurefor the reaction of OPD and H2O2 was followed using a Mb/Tris catalyst and an acetonitrile suspension. Like yesterday, the reaction was run in a beaker with a stir bar and the solution was filtered before taking a spectrum.

In addition reactions were run using Mb/Phosphate and Mb/Acetate in acetone suspension. Because the acetone corroded the plastic, samples 80mins-140mins are taken without filtering the sample.

Data

Mb/Tris in Acetonitrile

Mb Tris1 OPD H2O2 MeCN FILTERED WORKUP GRAPH.png

Note: The source was off during the 80mins measurement, so data was not available.

Mb Tris2 OPD H2O2 MeCN WORKUP GRAPH.png


Mb/Phosphate in Acetone

Mb Phosphate OPD H2O2 Acetone WORKUP GRAPH.png

Mb/Acetate in Acetone

Mb Acetate OPD H2O2 Acetone WORKUP GRAPH.png