User:Andrew W Long/Notebook/Synthesis of Lipid Modulators/2015/10/27

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Further Purification of AL2 with a focus on fraction 2

To do:

  • take supernatant of fraction 1 and run an MS scan (DONE)
  • run TLC of fraction 1 against fraction 2 (DONE)
    • There was a lot of smearing/streaking in the first trial. The sample was then further diluted (I think I overloaded the plate). There were not clean dots on the plate on the second trial (not perfectly circular like in the last plate).
  • filter the large amount of crude AL2 to remove dimers (complete), then run through the Buchi with a slower ramp up in polarity (DONE).