User:Andrew W Long/Notebook/Synthesis of Lipid Modulators/2015/10/07

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TLC Analysis and Bucci Separator

  1. TLC
  • Separation of EtOAc fraction was done using a 1:1 mixture of hexane and EtOAc. The plate showed 2 distinct and separate marks when 3 were suspected. Mass spectrometry was done on the two TLC fractions recovered from the plate.
    • The compound was not present in the upper fraction