Difference between revisions of "User:Samiye Yaman/Notebook/Lab 581/2012/11/02"

From OpenWetWare
< User:Samiye Yaman‎ | Notebook‎ | Lab 581‎ | 2012‎ | 11
Jump to: navigation, search
(Autocreate 2012/11/02 Entry for User:Samiye_Yaman/Notebook/Lab_581)
 
Line 10: Line 10:
  
  
 +
 +
==Objective==
  
 
==Description==
 
==Description==
 
*The course is designed by American University to experiment different aspects of PVOH films.
 
  
*During the course PVOH films with different molecular weight will be produced. Effects of cross-linking, addition of different molecules such as gluteraldehyde, different acids, porphrin will be also tested.
+
'''Part 1 '''
 +
 
 +
*Porphyrin film which was cross-linked on 19/10/2012 was placed in to a 1% HCL solution with a volume of 100mL.
 +
 
 +
'''Part 2: Prepare a porphyrin solution of 50micM'''
 +
 
 +
'''Part 3: UV-Vis'''
 +
 
 +
*Combination of 1 ml of salt/acid (50micM), 1 ml of 50 micM of porphyrin and 2 ml of HPLC water.
 +
 
 +
==Data==
 +
 
 +
'''Before placing porphyrin film in to 1 % HCl solution'''
 +
[[Image:2012-10-31_11.19.50.jpg|500px]]
 +
 
 +
 
 +
'''After placing porphyrin film into 1 % HCl solution'''
 +
 
 +
*Edges of the film become more green.
 +
 
 +
[[Image:2012-10-31_11.21.49.jpg|500px]]
 +
 
 +
 
 +
'''Porphyrin film with 2 drops of HCL, prepared on 24/10/2012'''
 +
 
 +
*Before cross-linking
 +
 
 +
*The film shrunk and look more brittle.
 +
 
 +
*More intense green color.
 +
 
 +
[[Image:2012-10-31_11.23.11.jpg|500px]]
 +
 
 +
==Notes==
 +
This area is for any observations or conclusions that you would like to note.
 +
 
 +
 
 +
Use categories like tags. Change the "Course" category to the one corresponding to your course. The "Miscellaneous" tag can be used for particular experiments, as instructed by your professor. Please be sure to change or delete this tag as required so that the categories remain well organized.
 +
 
 +
[[Category:Course]]
 +
[[Category:Miscellaneous]]
 +
 
 +
 
 +
 
 +
<!-- ##### DO NOT edit below this line unless you know what you are doing. ##### -->
 +
|}
  
*UV-Vis spectrum, Atomic Absorption spectrum, X-Ray, FTIR, DMA, ISE and many other instruments will be used to analyze the results.
+
__NOTOC__

Revision as of 09:19, 2 November 2012

BDLlogo notext lr.png Experimental Chemistry <html><img src="/images/9/94/Report.png" border="0" /></html> Main project page
<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>Previous entry<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>Next entry<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>



Objective

Description

Part 1

  • Porphyrin film which was cross-linked on 19/10/2012 was placed in to a 1% HCL solution with a volume of 100mL.

Part 2: Prepare a porphyrin solution of 50micM

Part 3: UV-Vis

  • Combination of 1 ml of salt/acid (50micM), 1 ml of 50 micM of porphyrin and 2 ml of HPLC water.

Data

Before placing porphyrin film in to 1 % HCl solution 2012-10-31 11.19.50.jpg


After placing porphyrin film into 1 % HCl solution

  • Edges of the film become more green.

2012-10-31 11.21.49.jpg


Porphyrin film with 2 drops of HCL, prepared on 24/10/2012

  • Before cross-linking
  • The film shrunk and look more brittle.
  • More intense green color.

2012-10-31 11.23.11.jpg

Notes

This area is for any observations or conclusions that you would like to note.


Use categories like tags. Change the "Course" category to the one corresponding to your course. The "Miscellaneous" tag can be used for particular experiments, as instructed by your professor. Please be sure to change or delete this tag as required so that the categories remain well organized.