Difference between revisions of "User:Samiye Yaman/Notebook/Lab 581/2012/11/02"

From OpenWetWare
< User:Samiye Yaman‎ | Notebook‎ | Lab 581‎ | 2012‎ | 11
Jump to: navigation, search
(Autocreate 2012/11/02 Entry for User:Samiye_Yaman/Notebook/Lab_581)
 
(Data)
(12 intermediate revisions by the same user not shown)
Line 10: Line 10:
  
  
 +
 +
==Objective==
  
 
==Description==
 
==Description==
 
*The course is designed by American University to experiment different aspects of PVOH films.
 
  
*During the course PVOH films with different molecular weight will be produced. Effects of cross-linking, addition of different molecules such as gluteraldehyde, different acids, porphrin will be also tested.
+
'''Part 1 '''
 +
 
 +
*Place the porphyrin film (with 2 drops of HCL), prepared on 24/10/2012, into a 6 molality of NaCl with 100ml of HPLC water.
 +
 
 +
*Place the NaCl solution in to a hot plate and wait until temperature raises to 70C.
 +
 
 +
*At 70C place the film into beaker.
 +
 
 +
 
 +
'''Part 2'''
 +
 
 +
*FTIR measurement for every film that has been prepared.
 +
 
 +
==Data==
 +
 
 +
'''Porphyrin film with 2 drops of HCL, prepared on 24/10/2012'''
 +
 
 +
'''*Before cross-linking'''
 +
 
 +
*The film shrunk and look more brittle.
 +
 
 +
*More intense green color.
 +
 
 +
[[Image:2012-10-31_11.23.11.jpg|500px]]
 +
 
 +
'''*After cross-linking'''
 +
 
 +
*The film expanded a little.
 +
 
 +
*Less intense green color and looked more reddish brown.
 +
 
 +
[[Image:2012-11-07_08.38.59.jpg|500px]]
 +
 
 +
 
 +
 
 +
'''FTIR Results'''
 +
 
 +
[[Image:1g22000PVOHcrosslinked.png|500px]]
 +
 
 +
 
 +
[[Image:1g22000PVOHH3PO4MaleicAcid.png|500px]]
 +
 
 +
[[Image:1g22000PVOHH3PO4MaleicAcidcrosslinked.png|500px]]
 +
 
 +
[[Image:1gPVOH22000H3PO4.png|500px]]
 +
 
 +
[[Image:1gPVOH100000.png|500px]]
 +
 
 +
[[Image:1gPVOH100000HCl.png|500px]]
 +
 
 +
[[Image:1gPVOH100000HClcrosslinked.png|500px]]
 +
 
 +
[[Image:Halfg22000PVOHgluteraldehyde.png|500px]]
 +
 
 +
[[Image:Halfg100000PVOHcrosslinked.png|500px]]
 +
 
 +
[[Image:HalfgPVOH2200.png|500px]]
 +
 
 +
[[Image:HalfgPVOH22000H3PO4.png|500px]]
 +
 
 +
[[Image:HalfgPVOH100000HCl.png|500px]]
 +
 
 +
[[Image:HalfgPVOH100000HClSuccinicAcid.png|500px]]
 +
 
 +
[[Image:OnetenthgPVOH22000.png|500px]]
 +
 
 +
[[Image:OnetenthgPVOH100000.png|500px]]
 +
 
 +
==Notes==
 +
This area is for any observations or conclusions that you would like to note.
 +
 
 +
 
 +
Use categories like tags. Change the "Course" category to the one corresponding to your course. The "Miscellaneous" tag can be used for particular experiments, as instructed by your professor. Please be sure to change or delete this tag as required so that the categories remain well organized.
 +
 
 +
[[Category:Course]]
 +
[[Category:Miscellaneous]]
 +
 
 +
 
 +
 
 +
<!-- ##### DO NOT edit below this line unless you know what you are doing. ##### -->
 +
|}
  
*UV-Vis spectrum, Atomic Absorption spectrum, X-Ray, FTIR, DMA, ISE and many other instruments will be used to analyze the results.
+
__NOTOC__

Revision as of 07:03, 14 November 2012

BDLlogo notext lr.png Experimental Chemistry <html><img src="/images/9/94/Report.png" border="0" /></html> Main project page
<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>Previous entry<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>Next entry<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>



Objective

Description

Part 1

  • Place the porphyrin film (with 2 drops of HCL), prepared on 24/10/2012, into a 6 molality of NaCl with 100ml of HPLC water.
  • Place the NaCl solution in to a hot plate and wait until temperature raises to 70C.
  • At 70C place the film into beaker.


Part 2

  • FTIR measurement for every film that has been prepared.

Data

Porphyrin film with 2 drops of HCL, prepared on 24/10/2012

*Before cross-linking

  • The film shrunk and look more brittle.
  • More intense green color.

2012-10-31 11.23.11.jpg

*After cross-linking

  • The film expanded a little.
  • Less intense green color and looked more reddish brown.

2012-11-07 08.38.59.jpg


FTIR Results

1g22000PVOHcrosslinked.png


1g22000PVOHH3PO4MaleicAcid.png

1g22000PVOHH3PO4MaleicAcidcrosslinked.png

1gPVOH22000H3PO4.png

1gPVOH100000.png

1gPVOH100000HCl.png

1gPVOH100000HClcrosslinked.png

Halfg22000PVOHgluteraldehyde.png

Halfg100000PVOHcrosslinked.png

HalfgPVOH2200.png

HalfgPVOH22000H3PO4.png

HalfgPVOH100000HCl.png

HalfgPVOH100000HClSuccinicAcid.png

OnetenthgPVOH22000.png

OnetenthgPVOH100000.png

Notes

This area is for any observations or conclusions that you would like to note.


Use categories like tags. Change the "Course" category to the one corresponding to your course. The "Miscellaneous" tag can be used for particular experiments, as instructed by your professor. Please be sure to change or delete this tag as required so that the categories remain well organized.