Difference between revisions of "User:Samiye Yaman/Notebook/Lab 581/2012/10/31"

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==Data==
 
==Data==
  
'''ISE results for sodium sulfate dilutions'''
+
'''Before placing porphyrin film in to 1 % HCl solution'''
 +
[[Image:2012-10-31_11.19.50.jpg|500px]]
  
*Dilution 1(1.25ppm)= -180mV
 
  
*Dilution 2(2.5ppm)=  -182.6mV
+
'''Right after placing porphyrin film into 1 % HCl solution'''
  
*Dilution 3(5ppm)  = -182.4mV
+
*Edges of the film become more green.
  
*Dilution 4(10ppm )= -177.4mV
+
[[Image:2012-10-31_11.21.49.jpg|500px]]
  
*Dilution 5(20ppm)= -174.6mV
+
'''48 hours after placing porphyrin film, prepared into 1 % HCl solution'''
  
 +
*The film became full green.(compared to the pictures on 31/10/2012)
  
*We decided detection limit was between dilution 1 and 2.
+
[[Image:2012-11-02_12.14.36.jpg|500px]]
 
 
*More negative number means less sodium ion in the solution.
 
 
 
*The porphyrin films prepared on 10/10/2012 had a yellowish green color. They were not clear as the other films.
 
  
 
==Notes==
 
==Notes==

Revision as of 10:28, 2 November 2012

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Objective

Description

Part 1

  • Porphyrin film which was cross-linked on 19/10/2012 was placed in to a 1% HCL solution with a volume of 100mL.

Part 2: Prepare a porphyrin solution of 50micM

Part 3: UV-Vis

  • Combination of 1 ml of salt/acid (50micM), 1 ml of 50 micM of porphyrin and 2 ml of HPLC water.

Data

Before placing porphyrin film in to 1 % HCl solution 2012-10-31 11.19.50.jpg


Right after placing porphyrin film into 1 % HCl solution

  • Edges of the film become more green.

2012-10-31 11.21.49.jpg

48 hours after placing porphyrin film, prepared into 1 % HCl solution

  • The film became full green.(compared to the pictures on 31/10/2012)

2012-11-02 12.14.36.jpg

Notes

This area is for any observations or conclusions that you would like to note.


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