Difference between revisions of "User:Puja Mody/Notebook/AU Biomaterials 572/2014/02/04"

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(Day 3)
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==Day 3==
 
* Goals:
 
# Prepare a Au:Hemoglobin solution using the method of protein- AuNP preparation found [[User:Puja Mody/Notebook/AU Biomaterials 572/2014/01/28|Here]] (It is the same as the Au-BSA solutions prepared). These samples will be used for comparison against the new method preparation done today. 
 
#Prepare two Magnetitic and hemoglobin solutions. The first  following the protocol described on [[User:Puja Mody/Notebook/AU Biomaterials 572/2014/01/29|Wednesday]]. Everything will once again be constantly de-gassed with nitrogen using the Schlenk line. And the second following the same ratio and protocol listed on [[User:Puja Mody/Notebook/AU Biomaterials 572/2014/01/28|Tuesday]]. The preparation of these two samples will allow for comparison in the future.
 
#Filter the Magnetite:Au-BSA solutions from [[User:Puja Mody/Notebook/AU Biomaterials 572/2014/01/29|Last week]] using a Whatman filter paper with a pore size of 20-25μ. This filtrate will be dried and analyzed using DSC, FTIR and XRD.
 
#Potentiall place some of the prepared fibers in water in order to test their stability. 
 
#Test magnetic property of the fibers using a magnet/magnetometer.
 
#Centrifuge recollected solution for future AA analysis.
 
 
 
==Procedure==
 
*Made Hemoglobin+ Magnetite solution. Bubbled through nitrogen for 4 hours
 
*Centrifuge the Hemoglobin- magnetite- gold samples
 
*made 4 different ratios of hemoglobin and magnetite
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
 
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Latest revision as of 18:48, 19 April 2014

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