User:Paul Rothenberg/Notebook/Pauls Notebook/2013/06/12: Difference between revisions

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==Reaction of OPD+H<sub>2</sub>O<sub>2</sub> with Mb/Citrate Catalyst in Acetone Suspension==
==Reaction of OPD+H<sub>2</sub>O<sub>2</sub> with Mb/PhosphateCatalyst in Acetone Suspension==
 
We are going to run the same reaction as yesterday, but, the samples will be centrifuged before a spectrum is taken. Hopefully, the results will be more consistent than yesterday's.
 
 
We let the reaction run for 20 minute intervals, took a 1 mL sample, and centrifuged it for 1 minute at 13,200 rpm.
 
<b>Data:</b>


We are going to run the same reaction as yesterday, just switching out the buffered Mb solutions. Hopefully, the results will be more consistent than yesterday's. We will not filter the solution; just remove a 1 mL sample and take a spectrum of it.  
[[Image:Mb_Phosphate_OPD_H2O2_Acetone_RERUN_GRAPH.png|750px]]


==Reaction of OPD+H<sub>2</sub>O<sub>2</sub> with Mb/Acetate Catalyst in Acetone Suspension==


[[Image:Mb_Acetate_OPD_H2O2_Acetone_RERUN_WORKUP_GRAPH.png|750px]]




==Reaction of OPD+H<sub>2</sub>O<sub>2</sub> with Mb/Citrate Catalyst in Acetone Suspension==


==Reaction of OPD+H<sub>2</sub>O<sub>2</sub> with Mb/TrisCatalyst in Acetone Suspension==
[[Image:Mb_Citrate_OPD_H2O2_Acetone_WORKUP_GRAPH.png|750px]]
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Revision as of 09:27, 8 July 2013

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Reaction of OPD+H2O2 with Mb/PhosphateCatalyst in Acetone Suspension

We are going to run the same reaction as yesterday, but, the samples will be centrifuged before a spectrum is taken. Hopefully, the results will be more consistent than yesterday's.


We let the reaction run for 20 minute intervals, took a 1 mL sample, and centrifuged it for 1 minute at 13,200 rpm.

Data:

Reaction of OPD+H2O2 with Mb/Acetate Catalyst in Acetone Suspension


Reaction of OPD+H2O2 with Mb/Citrate Catalyst in Acetone Suspension


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