Difference between revisions of "User:Paul Rothenberg/Notebook/Pauls Notebook/2013/06/12"

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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span>
 
|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span>
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
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|style="background-color: #F2F2F2" align="center"|[[File:Report.png|frameless|link={{#sub:{{FULLPAGENAME}}|0|-11}}]][[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|[[File:Resultset_previous.png|frameless|link={{#lnpreventry:{{FULLPAGENAME}}}}]][[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]][[File:Resultset_next.png|frameless|link={{#lnnextentry:{{FULLPAGENAME}}}}]]}}
 
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==Reaction of OPD+H<sub>2</sub>O<sub>2</sub> with Mb/Citrate Catalyst in Acetone Suspension==
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==Reaction of OPD+H<sub>2</sub>O<sub>2</sub> with Mb/PhosphateCatalyst in Acetone Suspension==
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We are going to run the same reaction as yesterday, but, the samples will be centrifuged before a spectrum is taken. Hopefully, the results will be more consistent than yesterday's.
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We let the reaction run for 20 minute intervals, took a 1 mL sample, and centrifuged it for 1 minute at 13,200 rpm.
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<b>Data:</b>
  
We are going to run the same reaction as yesterday, just switching out the buffered Mb solutions. Hopefully, the results will be more consistent than yesterday's. We will not filter the solution; just remove a 1 mL sample and take a spectrum of it.  
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[[Image:Mb_Phosphate_OPD_H2O2_Acetone_RERUN_GRAPH.png|750px]]
  
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==Reaction of OPD+H<sub>2</sub>O<sub>2</sub> with Mb/Acetate Catalyst in Acetone Suspension==
  
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[[Image:Mb_Acetate_OPD_H2O2_Acetone_RERUN_WORKUP_GRAPH.png|750px]]
  
  
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==Reaction of OPD+H<sub>2</sub>O<sub>2</sub> with Mb/Citrate Catalyst in Acetone Suspension==
  
==Reaction of OPD+H<sub>2</sub>O<sub>2</sub> with Mb/TrisCatalyst in Acetone Suspension==
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[[Image:Mb_Citrate_OPD_H2O2_Acetone_WORKUP_GRAPH.png|750px]]
 
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Latest revision as of 22:45, 26 September 2017

Owwnotebook icon.png Project name Report.pngMain project page
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Reaction of OPD+H2O2 with Mb/PhosphateCatalyst in Acetone Suspension

We are going to run the same reaction as yesterday, but, the samples will be centrifuged before a spectrum is taken. Hopefully, the results will be more consistent than yesterday's.


We let the reaction run for 20 minute intervals, took a 1 mL sample, and centrifuged it for 1 minute at 13,200 rpm.

Data:

Mb Phosphate OPD H2O2 Acetone RERUN GRAPH.png

Reaction of OPD+H2O2 with Mb/Acetate Catalyst in Acetone Suspension

Mb Acetate OPD H2O2 Acetone RERUN WORKUP GRAPH.png


Reaction of OPD+H2O2 with Mb/Citrate Catalyst in Acetone Suspension

Mb Citrate OPD H2O2 Acetone WORKUP GRAPH.png