Difference between revisions of "User:Paul Rothenberg/Notebook/Pauls Notebook/2012/10/10"

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(10 October 2012)
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|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span>
|style="background-color: #EEE"|[[Image:owwnotebook_icon.png|128px]]<span style="font-size:22px;"> Project name</span>
|style="background-color: #F2F2F2" align="center"|<html><img src="/images/9/94/Report.png" border="0" /></html> [[{{#sub:{{FULLPAGENAME}}|0|-11}}|Main project page]]<br />{{#if:{{#lnpreventry:{{FULLPAGENAME}}}}|<html><img src="/images/c/c3/Resultset_previous.png" border="0" /></html>[[{{#lnpreventry:{{FULLPAGENAME}}}}{{!}}Previous entry]]<html>&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;&nbsp;</html>}}{{#if:{{#lnnextentry:{{FULLPAGENAME}}}}|[[{{#lnnextentry:{{FULLPAGENAME}}}}{{!}}Next entry]]<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>}}
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Latest revision as of 21:07, 26 September 2017

Owwnotebook icon.png Project name Report.pngMain project page
Resultset previous.pngPrevious entry      Next entryResultset next.png

10 October 2012

  • 1. UV-Vis spectrum was calibrated with DMF. System checks were performed, and a baseline was run from 800-200 nm.
  • 2. DMF was used as a baseline, and run from 800-200 nm. The file was saved as a .spc file and a .txt file to dropbox
  • 3. DMF was then run under Fluorescence, and the file was saved to dropbox
  • 4. The 4μM NiPPIX was run under UV-VIS and Fluorescence
  • 5. The 2μM NIPPIX was run under UV-VIS and Fluorescence
  • 6. The 0.5μM NiPPIX was run under UV-VIS and Fluorescence
  • Fluorescence revealed two peaks in the NiPPIX, at approximately 590 nm and 640 nm, indicating that there is a presence of porphyrin with no nickel and nickel porphyrin. The synthesis needs to be reperformed until the second peak is not present under fluorescence.

Absorbance of UV-Vis Graph.JPG

Fluorescence of NiPPIX Graph.JPG