User:Moira M. Esson/Notebook/CHEM-581/2013/04/10: Difference between revisions
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==DSC Analysis== | ==DSC Analysis== | ||
*The general protocol for DSC analysis was followed. | |||
* Specific DSC parameters ato analyze the following PVA/clay samples included the following: | |||
# Equilibrate sample at ~ -40°C | |||
# Ramp sample temperature up from 20-240°C | |||
# Ramp sample temperature down from 20-(-40°C) | |||
# Repeat segment #2 again | |||
Table 2. DSC samples information | |||
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{| {{table}} | {| {{table}} | ||
| align="center" style="background:#f0f0f0;"|'''Sample Name''' | | align="center" style="background:#f0f0f0;"|'''Sample Name''' | ||
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| 50:50 PVOH 130K 50% CEC NaMT w/ Bu<sub>3</sub>HdP<sup>+</sup>||3.04||49.95 | | 50:50 PVOH 130K 50% CEC NaMT w/ Bu<sub>3</sub>HdP<sup>+</sup>||3.04||49.95 | ||
|} | |} | ||
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* | *The following data samples will be collected during the next session. | ||
*Any previously run samples that were unable to be analyzed(described [[User:Moira_M._Esson/Notebook/CHEM-581/2013/04/05|2013/04/05]] were also re-run and will be collected during the next session. | |||
==Notes== | ==Notes== |
Revision as of 07:43, 15 April 2013
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Objectives
Film Preparation
Pressure Testing
DSC Analysis
# Equilibrate sample at ~ -40°C # Ramp sample temperature up from 20-240°C # Ramp sample temperature down from 20-(-40°C) # Repeat segment #2 again Table 2. DSC samples information
Notes
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