Difference between revisions of "User:Melissa Novy/Notebook/CHEM-581/2012/10/26"

From OpenWetWare
< User:Melissa Novy‎ | Notebook‎ | CHEM-581‎ | 2012‎ | 10
Jump to: navigation, search
(Autocreate 2012/10/26 Entry for User:Melissa_Novy/Notebook/CHEM-581)
 
(fix raw html help text)
 
(2 intermediate revisions by one other user not shown)
Line 10: Line 10:
 
<!-- ## END search column  ## -->
 
<!-- ## END search column  ## -->
 
|-  
 
|-  
|colspan="2" style="background-color: #F2F2F2;" align="right"|[[{{FULLPAGENAME}}/Entry_Base|Customize your entry pages]] [[Help:Notebook/Project_Base/Customize_entry_page|<html><img src="/images/a/aa/Help.png" border="0" /></html>]]
+
|colspan="2" style="background-color: #F2F2F2;" align="right"|[[{{FULLPAGENAME}}/Entry_Base|Customize your entry pages]] [[Image:Help.png|frameless|link=Help:Notebook/Project_Base/Customize_entry_page]]
 
|-  
 
|-  
 
|colspan="2"|
 
|colspan="2"|
 
<!-- ##### DO NOT edit above this line unless you know what you are doing. ##### -->
 
<!-- ##### DO NOT edit above this line unless you know what you are doing. ##### -->
==Entry title==
+
==Objectives==
* Insert content here...
+
* Crosslink PVOH(22K) + porphyrin films.
 +
* Analyze NaMT-CuSO<sub>4</sub> exchanged solutions with atomic absorption spectroscopy.
 +
 
 +
==Crosslinking PVOH Films==
 +
* The following films were crosslinked:
 +
** PVOH(22K) 1.0073 g, 1 mL GA, 1 mL porphyrin
 +
** PVOH(22K) 1.05225 g, 1 mL GA, 1 mL porphyrin
 +
** PVOH(22K) 1.02114 g, 0.5 mL GA, 1 mL porphyrin, HCl
 +
** PVOH(22K) 1.0067 g, 1 mL GA, 1 mL porphyrin, HCl
 +
* Please refer to [[User:Moira_M._Esson/Notebook/CHEM-581/2012/10/26|Moira Esson's entry]] for crosslinking data and observations.
 +
 
 +
==Atomic Absorption on NaMT-CuSO<sub>4</sub> Exchanged Solutions==
 +
* CuSO<sub>4</sub> standard solutions of 0.1, 0.5, 1, 2, and 3 ppm were prepared.
 +
* Please refer to [[User:Karlena_L._Brown/Notebook/PVOH_Research/2012/10/19|Karlena Brown's entry]] for AAS observations.
 +
{| {{table}}
 +
| align="center" style="background:#f0f0f0;"|'''Sample []'''
 +
| align="center" style="background:#f0f0f0;"|'''Initial [Cu] [ppm]'''
 +
| align="center" style="background:#f0f0f0;"|'''Abs. []'''
 +
| align="center" style="background:#f0f0f0;"|'''Actual [Cu] [ppm]'''
 +
|-
 +
| 1 min NaMT-CuSO4||7.4||0.0043||5.6399
 +
|-
 +
| ||10||0.0062||7.0191
 +
|-
 +
| 5 min NaMT-CuSO4||7.4||0.0035||5.6942
 +
|-
 +
| ||10||0.006||7.0956
 +
|-
 +
| 10 min NaMT-CuSO4||7.4||0.0037||4.5058
 +
|-
 +
| ||10||0.0048||5.633
 +
|-
 +
| 1 min 100%CEC NaMT-CuSO4||7.4||0.0068||7.0789
 +
|-
 +
| ||10||0.0095||9.0063
 +
|-
 +
| 5 min 100%CEC NaMT-CuSO4||7.4||0.0064||6.8131
 +
|-
 +
| ||10||0.0079||9.0342
 +
|-
 +
| 10 min 100%CEC NaMT-CuSO4||7.4||0.004||6.4207
 +
|-
 +
| ||10||0.0048||9.1566
 +
|-
 +
| 1 min 50%CEC NaMT-CuSO4||7.4||0.0053||7.001
 +
|-
 +
| ||10||0.0049||9.03
 +
|-
 +
| 5 min 50%CEC NaMT-CuSO4||7.4||0.0031||6.8117
 +
|-
 +
| ||10||0.0058||8.8755
 +
|-
 +
| 10 min 50%CEC NaMT-CuSO4||7.4||0.0039||6.9077
 +
|-
 +
| ||10||0.0044||8.6918
 +
|}
  
  

Latest revision as of 18:52, 23 September 2017

<!-- sibboleth --><div id="lncal1" style="border:0px;"><div style="display:none;" id="id">lncal1</div><div style="display:none;" id="dtext"></div><div style="display:none;" id="page">User:Melissa Novy/Notebook/CHEM-581/2012/10/26</div><div style="display:none;" id="fmt">yyyy/MM/dd</div><div style="display:none;" id="css">OWWNB</div><div style="display:none;" id="month"></div><div style="display:none;" id="year"></div><div style="display:none;" id="readonly">Y</div></div>

BDLlogo 300.png <sitesearch>title=Search this Project</sitesearch>

Customize your entry pages Help.png

Objectives

  • Crosslink PVOH(22K) + porphyrin films.
  • Analyze NaMT-CuSO4 exchanged solutions with atomic absorption spectroscopy.

Crosslinking PVOH Films

  • The following films were crosslinked:
    • PVOH(22K) 1.0073 g, 1 mL GA, 1 mL porphyrin
    • PVOH(22K) 1.05225 g, 1 mL GA, 1 mL porphyrin
    • PVOH(22K) 1.02114 g, 0.5 mL GA, 1 mL porphyrin, HCl
    • PVOH(22K) 1.0067 g, 1 mL GA, 1 mL porphyrin, HCl
  • Please refer to Moira Esson's entry for crosslinking data and observations.

Atomic Absorption on NaMT-CuSO4 Exchanged Solutions

  • CuSO4 standard solutions of 0.1, 0.5, 1, 2, and 3 ppm were prepared.
  • Please refer to Karlena Brown's entry for AAS observations.
Sample [] Initial [Cu] [ppm] Abs. [] Actual [Cu] [ppm]
1 min NaMT-CuSO4 7.4 0.0043 5.6399
10 0.0062 7.0191
5 min NaMT-CuSO4 7.4 0.0035 5.6942
10 0.006 7.0956
10 min NaMT-CuSO4 7.4 0.0037 4.5058
10 0.0048 5.633
1 min 100%CEC NaMT-CuSO4 7.4 0.0068 7.0789
10 0.0095 9.0063
5 min 100%CEC NaMT-CuSO4 7.4 0.0064 6.8131
10 0.0079 9.0342
10 min 100%CEC NaMT-CuSO4 7.4 0.004 6.4207
10 0.0048 9.1566
1 min 50%CEC NaMT-CuSO4 7.4 0.0053 7.001
10 0.0049 9.03
5 min 50%CEC NaMT-CuSO4 7.4 0.0031 6.8117
10 0.0058 8.8755
10 min 50%CEC NaMT-CuSO4 7.4 0.0039 6.9077
10 0.0044 8.6918