Difference between revisions of "User:Megan L. Channell/Notebook/Masters Research/2013/10/03"

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(Protocol)
 
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# Once both fully dissolved, the zinc acetate was added to the organic solution
 
# Once both fully dissolved, the zinc acetate was added to the organic solution
 
#Solution stirred for 2.5 hours
 
#Solution stirred for 2.5 hours
 +
#Filter out solid
 +
 +
*left for the day, so left in the hood
 +
 +
**Next time
 +
#Save ~1 mg of solid
 +
#Put precipitate in 250 mL of DMF and left in hood with watch glass on
  
 
==Results==
 
==Results==

Latest revision as of 14:10, 3 October 2013

Owwnotebook icon.png Project name <html><img src="/images/9/94/Report.png" border="0" /></html> Main project page
Next entry<html><img src="/images/5/5c/Resultset_next.png" border="0" /></html>

MOF-5 Synthesis

  • Synthesize MOF-5 by using the protocol from FIX THIS (room temp. synthesis of metal-organic frameworks:MOF-5..... Tranchemontagne...)

Protocol

  1. 5.0065 g of terephthalic acid and 8.5 mL of triethylamine dissolved in 400 mL of DMF
  2. 16.881 g of zinc acetate dissolved in 500 mL of DMF
  3. Once both fully dissolved, the zinc acetate was added to the organic solution
  4. Solution stirred for 2.5 hours
  5. Filter out solid
  • left for the day, so left in the hood
    • Next time
  1. Save ~1 mg of solid
  2. Put precipitate in 250 mL of DMF and left in hood with watch glass on

Results