Difference between revisions of "User:Matt Hartings/Notebook/Photosynthesis/2013/01/22"

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(Autocreate 2013/01/22 Entry for User:Matt_Hartings/Notebook/Photosynthesis)
 
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==Objective==
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==MOF==
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Abigail and I are doing a new MOF synthesis today with [https://macrocyclics.com/shop/product_info.php?cPath=2&products_id=69&osCsid=f9126a59350aa546308b0a8c52d5e244 DO2A].
  
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Plan: 50 mg of DO2A (MW = 424.2) + 59.0 mg of Zn(Acetate)2·4H2O (MW = 291.5) ratio of 7 Zn for each 3 DO2A. This is from the ratio's from the papers for the synthesis of MOF-5 (4Zns:3ligands) but each of our ligands needs an extra Zn for the middle of the macrocycle.
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Actual:
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51.3mg of DO2A and 59.8mg of Zn(Acetate)2·4H2O. Add 2mL of diethylformamide. Put in oven (85C) at 11:23 am.
  
 
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Revision as of 12:51, 22 January 2013

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MOF

Abigail and I are doing a new MOF synthesis today with DO2A.

Plan: 50 mg of DO2A (MW = 424.2) + 59.0 mg of Zn(Acetate)2·4H2O (MW = 291.5) ratio of 7 Zn for each 3 DO2A. This is from the ratio's from the papers for the synthesis of MOF-5 (4Zns:3ligands) but each of our ligands needs an extra Zn for the middle of the macrocycle.

Actual: 51.3mg of DO2A and 59.8mg of Zn(Acetate)2·4H2O. Add 2mL of diethylformamide. Put in oven (85C) at 11:23 am.